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Cadmium bis(tetrahydroborate) has been prepared from dimethyl cadmium and H 3 B · THF in tetrahydrofuran. Low temperature  113 Cd NMR spectra recorded for THF, monoglyme and diglyme solutions show a septet with  1 J( 113 Cd 1 H) = 273 Hz. This proves that the BH 4 ⁻ groups are bound to the metal centre via triple hydride bridges. Reaction of Cd(BH 4 ) 2  with LiBH 4  yields LiCd(BH 4 ) 3  quantitatively in diglyme solution.

Metal Tetrahydroborates and Tetrahydroborato Metalates, 17 / Bonding in Cadmium Bis(tetrahydroborate), and the Reaction with Lithium Tetrahydroborate