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Red crystals of the title compound have been prepared from pyridine, potassium dithiosquarate and copper(II) sulfate in water at pH 5. 1 contains an infinite zigzag chain of Cu I  atoms, which extends orthogonally through a stacked structure formed by pyridinium and dithiosquarate ions. The Cu I  atoms are tetrahedrally and trigonally coordinated by sulfur atoms. The Cu···Cu distances are 257.3(8), 262.1(8) and 276.4(8) pm. Crystal data: triclinic, space group P 1̄, a = 7.92(2), b = 10.52(2), c = 14.39(2) pm, α = 102.5(2), β = 104.1 (2), γ = 100.6(2)°, V = 1100.34 nm 3 , Ζ = 4; 3102 reflections, R = 0.103

zeitschrift für naturforschung b

Notizen: (Pyridinium)[(1,2-dithioquadratato)-cuprat(I)]hydrat, eine Verbindung mit einer Cu I ···Cu I -Zickzackkette / (Pyridinium)[( 1,2-dithiosquarato)-cuprate(I)]hydrate, a Compound with a Cu I ···Cu I -Zigzag Chain