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Ethylenediammonium Hydridotrioxophosphate(2–) [H 3 NCH 2 CH 2 NH 3 ][PHO 3 ] is formed by slow oxidation of white phosphorus by oxygen in ethylendiamine. It crystallizes in the space group Pbca with a = 1570.6(4) pm, b = 676.9(5) pm, c = 1267.8(4) pm and Z = 8 formula units in the unit cell. The structure is built from ethylenediammonium dications and tetrahedral phosphonate dianions, linked by O ··· H–N bonds (d̄(O…N) = 275.8 pm). The bond distances are d̄(P–O) = 151.8 pm, d̄(P–H) = 136.9 pm, d̄(N–C) = 148.3 pm and d̄(C–C) = 151.0 pm.

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Bildung und Kristallstruktur von Ethylendiammonium-hydridotrioxophosphat(2–) [H 3 NCH 2 CH 2 NH 3 ][PHO 3 ] a  / Formation and Crystal Structure of Ethylenediammonium Hydridotrioxophosphate(2—) [H 3 NCH 2 CH 2 NH 3 ][PHO 3 ]