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Using a modified cyanide process RbAu(CN) 2  was synthesized by the reaction of gold powder with RbOH, O 2  and liquid HCN. The colourless crystals are monoclinic, space group C2/c, with a = 18.450(3), b = 8.998(2), c = 13.418(2) Å, β = 108.0(9)° and Z = 16. The structure could be solved by Patterson and standard direct methods and refined to R = 0.035 and Rw = 0.034, respectively, for 857 absorption-corrected unique reflections. The structure comprises layers of linear [Au(CN) 2 ] -  groups, in which gold atoms are arranged in four- and eightmembered rings. The stacking of the layers with a sequence ABAB creates different kinds of holes which are occupied by the rubidium ions.

Darstellung und Kristallstruktur von Rubidiumdicyanoaurat(I), RbAu(CN) 2 / Synthesis and Crystal Structure of Rubidium Dicyanoaurate(I), RbAu(CN) 2