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Crystalline 3-O-acetyl-2,4-O-phenylboranediyl-β-D-ribopyranosyl bromide (5) is prepared by an easy four-step synthesis from D-ribose (1), the first three steps of which are realised in an one-pot manner. 5 reacts stereoselectively with sodium methoxide and phenoxide to give the pure methyl and phenyl a-D-ribopyranosides 7 a and 7 b after deboronation and deacetylation.

Synthesis and Stereoselective Glycosylations of 3-O-Acetyl-2,4-O-phenylboranediyl-β-D-ribopyranosyl Bromide