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Cationic halfsandwich-type complexes of sulfur dioxide, [C 5 R 5 M(PR 3 )2(SO 2 )] +  (R = H, Me, M = Fe, Ru, (PR 3 ) 2  = mono- or bidentate phosphorus ligands) and [C 5 Me 5 Fe(CO)(PR 3 )(SO 2 )] + , are obtained by ligand exchange from labile cationic (M = Fe) or neutral (M = Ru) precursors. The new compounds are characterized by IR,  1 H 13  1 H,  13 C and  31 P NMR spectroscopy. Their stability increases with increasing electron density at the metal.

zeitschrift für naturforschung b

Kationische Schwefeldioxid-Komplexe des Eisens und Rutheniums vom Halbsandwich-Typ [1] / Cationic Halfsandwich-Type Sulfur Dioxide Complexes of Iron and Ruthenium [1]