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The preparations and characterizations of compounds SCl 2 F + MF 6 ~ (M = As, Sb) are reported. They are yellowish hydrolysable solids, with a strong tendency towards symmetrization in solution. The mass spectra data indicate the formation of SCl 2 F 2  on thermolysis. The series of SCl n F 3-n  + -cations (n = 0—3) is now complete, and a comprehensive discussion of the spectroscopic data is given.

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Darstellung von SCl 2 F + MF 6 ~ (M = As, Sb) und zusammenfassende Betrachtung der Kationen SCl n F 3-n  +  (n = 0-3) [1] / Preparation of SCl 2 F + MF 6 ~ (M = As, Sb) and a Comprehensive Discussion of the Cations SCl n F 3-n  +  (n = 0-3) [1]