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Using 293 K diffractometer intensity data, the structure of [H 3 N(CH 2 )3NH 3 ]SbCl 5  has been determined by single crystal X-ray technique and refined to a final R w  of 0.026. The colorless crystals are monoclinic (space group P2 1 /c) with a = 10.1338(5), b = 11.4623(7), c = 11.3668(6) Å, β = 113.52(5)° and Ζ = 4. The structure contains ψ-octahedral SbCl 5  2-  anions. A center of symmetry connects two anions forming a (Sb 2 Cl 10 ) 4-  unit with rather long Sb—Cl distances for the bridging Cl-atoms (2.92 and 3.68 A, respectively).

Notizen: Darstellung und Kristallstruktur von [H 3 N(CH 2 ) 3 NH 3 ]SbCl 5 / Preparation and Crystal Structure of [H 3 N(CH 2 ) 3 NH 3 ]SbCl 5