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All components of the two series Cs 2 [PtF„ 35 Cl 6-n ] and Cs 2 [PtF n  37 Cl 6-n ], including the pairs of geometric isomers for n = 2,3, 4, have been prepared and isolated by ion exchange chromatography on DEAE cellulose. The highly resolved low temperature (80 K) IR and Raman spectra of the pure isotopomers show distinctive isotopic shifts for different vibrational modes up to 10 cm -1 . The excellent agreement of the observed values with Teller-Redlich calculations verifies the assignment of all stretching and especially of the narrow deformation bands. For transcomplexes containing  35 Cl-Pt- 37 Cl axes, the lowered symmetry affects the restriction of the rule of mutual exclusion

zeitschrift für naturforschung b

Darstellung und Schwingungsspektren der  35 Cl/ 37 Cl-markierten Fluoro-Chloro-Platinate(IV) / Preparation and Vibrational Spectra of  35 Cl/ 37 Cl Labelled Fluoro-Chloro-Platinates(IV)