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Triphenylboron adducts of 2- and 3-hydroxyalkyl isocyanides spontaneously undergo intramolecular cyclization to give oxazolidin-2-ylidene and perhydrooxazin-2-ylidene boron complexes, respectively. The same compounds are obtained by methanolysis of the stable species Ph 3 B-CNCR 1 R 2 CR 3 R 4 -OSiMe 3  (R 1 , R 2 , R 3 , R 4  = H, alkyl) (2a-i) and Ph 3 B-CN(CH 2 ) 3 -OSiMe 3  (2j)IR,  1 H NMR,  13 C{H} NMR. and mass spectra of the new compounds are reported.

zeitschrift für naturforschung b

Bor-stabilisierte N,O-Carbene, I Triphenylbor-Addukte von Siloxy-und Hydroxyalkylisocyaniden und spontane At-Ylid-Bildung / Boron-Stabilized N.O-Carbenes, I Triphenylboron Adducts of Siloxy- and Hydroxyalkyl Isocyanides and Spontaneous Formation of Ate-Ylids