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The crystal structure of calcium azide dihydrate trans-bicyclo-[4.4.0]-1,4,6.9-tetraazadecane has been determined by single crystal X-ray diffraction at 100 K. [Ca(N 3 ) 2 (H 2 O) 2  (C 6 H 14 N 4  crystallizes in the orthorhombic space group Pnma, Z = 4. with a - 1396.6(5), b = 1407.1(5), c = 712.2(2) pm. Calcium is hexacoordinated to four azide groups and two water molecules. The elongated octahedra are linked via μ(1,3)-bridging azide ions to form monolayers parallel to the ac-plane. The C 6 H 14 N 4  molecules are arranged between these layers.

Die Kristallstruktur von [Ca(N 3 ) 2 (H 2 O) 2 ] · C 6 H 14 N 4 bei 100 K /The Crystal Structure of [Ca(N 3 ) 2 (H 2 O) 2 ] · C 6 H 14 N 4 at 100 K