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N-Acyl dimesylamines RC(O)N(SO 2 CH 3 ) 2  (3) have been prepared by reacting solid KN(SO 2 CH 3 ) 2  with neat liquid RC(O)Cl at 70-90 °C [R = C 2 H 5 , (CH 3 ) 2 CH, (CH 3 ) 3 C-CH 2  , CH 2 Cl, CHCl 2 ] or solutions of AgN(SO 2 CH 3 ) 2  in methyl cyanide with RC(O)Cl at room temperature [R = (CH 3 ) 3 C, CH 2 Cl, CHCl 2 , CCl 3  , C 6 H 5  , CH 2 =CH]. Addition of chlorine or bromine to 3 (R = CH 2  = CH) affords the corresponding compounds 3 with R = CH 2 Cl-CHCl and CH 2 Br-CHBr, respectively. By hydrolysis of 3 (R = CCl 3 ), CCl 3 C(O)NHSO 2 CH 3  (5) is obtained. The new compounds 3 and 5 are characterized by spectroscopic (NMR, MS) and analytical methods.

zeitschrift für naturforschung b

Polysulfonylamine, XII [1]. N-Acyl-dimesylamine (N.N-Dimesyl-carbonsäureamide) / Polysulfonylamines, XII [1]. N-Acyl Dimesylamines (Carboxylic Acid N.N-Dimesylamides)