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The crystal structure of [AsPh 4 ] 2 [Pb(N 3 ) 6 ] 2-  has been determined by X-ray diffraction. The structure of [Pb(N 3 ) 6 ] 2-  (C i  symmetry) is analogous to that of [Sn(N 3 ) 6 ] 2-  with covalent Pb-N bonds (222-226 pm) and angles Pb-N-N between 115 and 121°. Irridiation (daylight) of [AsPh 4 ] 2 [Pb(N 3 ) 6 ] in solution gives AsPh 4 [Pb(N 3 ) 3 ].

Pseudohalogeno Metal Compounds, LXXI [1] Hexaazidoplumbate(IV). Crystal Structure of [AsPh 4 ] 2 [Pb(N 3 ) 6 ]