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The crystal structure of Na 5 SnSb 3  (monoclinic, P2 1 /c, a = 1859.4(6), b = 918.1(4), c = 1249.3(5) pm, β = 98.3°, Z = 8) contains SnSb 4  tetrahedra which form chains by sharing common vertices. Isolated tetrahedral units SnSb 4  8-  are present in the crystal structure of K 8 SnSb 4  (cubic, Fd3m, a = 1627.9(3) pm, Z = 8). The compounds are in agreement with the Zintl concept.

Na 5 SnSb 3 und K 8 SnSb 4 , zwei neue Zintlphasen mit tetraedrischen SnSb 4 -Baueinheiten