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PPh 3 Me[HSO 4 ] was prepared by the reaction of (PPh 3 Me)I with silver sulfate in aqueous solution. OPPh 2 Me and benzene being the by-products. The title compound was characterized by its IR spectrum as well as by an X-ray structure determination (1730 observed independent reflexions, R = 0.043). Crystal data: a = 910.4(3). b = 1587.8(4), c = 1294.2(6) pm, β = 105.52(3)°. space group P2 1 /c, Z = 4. The structure consists of PPh3Me ⊕  cations and of HOSO 3  ⊖  ions that are associated via strong hydrogen bonds to dimeric centrosymmetric units.

Notizen: Synthese und Kristallstruktur von PPh 3 Me[HSO 4 ]/ Synthesis and Crystal Structure of PPh 3 Me[HSO 4 ]