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The crystal structure of the carbamoyl complex [(CO) 4 FeC(O)NMe 2 ][C(NMe 2 ) 3 ] (1) is described. It crystallizes in the triclinic space group PI (a = 7.876(3), b = 10.098(3), c = 12.067(5)Å, α = 94.25(3), β = 90.94(3), γ = 97.30(3)°, Z = 2) and consists of independent ions. The cation has a planar CN 3  array with sp 2  hybridized C and N atoms. The carbamoyl group of the anion occupies an axial position in the trigonal bipyramidal environment of the iron atom.

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[Fe(CO) 4 C(O)NMe 2 ][C(NMe 2 ) 3 ]; die erste Strukturbestimmung einer Organometallverbindung mit dem Carbeniumion [C(NMe 2 ) 3 ] + / [Fe(CO) 4 C(O)NMe 2 ][C(NMe 2 ) 3 ]; the First Structure Determination on an Organometallic Compound with the Carbenium Ion [C(NMe 2 ) 3 ] +