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A phase transfer reaction between the title ketones, sodium trichloroacetate, and an alkyl halide leads to 2a, b, 4, or 5. Whereas these com-pounds are fragmented by NaOH, sodium meth-oxide/methylmalonate/methanol give compound 8 from 5 in a complex series of consecutive rearrange-ments.

zeitschrift für naturforschung b

Durch Trichloracetat ausgelöste Alkylierungen von Trichlormethylketonen und eine komplexe Folgereaktion [1] / Alkylations of Trichloromethylketones Effected by Trichloroacetate and a Complex Consecutive Reaction [1]