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The compounds La 2 TaO 4 CL 3  and Ce 2 TaO 4 CL 3  have been prepared by reacting SECL 3  with SETaO 4  (SE = La, Ce) in evacuated silica ampoules. Single crystals of La 2 TaO 4 CL were obtained by chemical transport reaction (1100→1000 °C) using chlorine as transport agent. The crystal structure of La 2 TaO 4 Cl 3  has been refined with single crystal data (Pmmn; a = 15.528(1) Å. b = 3.9395(2) Å, c = 18.132(2) Å; Z = 6; R = 8.53%, R w  = 6.10%). Main building units are TaO 5  trigonal bipyramides and two- or threefold capped trigonal prisms around La.

La 2 TaO 4 Cl 3 — ein neues Oxochlorotantalat mit TaO 5 -Baugruppen / La 2 TaO 4 Cl 3 - a New Oxochlorotantalate with TaO 5 Building Units