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Reaction of 1,3,5-tris(dimethylamino)benzene (TDMAB) with iodine in solution gives dark red needles of a compound (1) with stoichiometry C 24 H 42 I 6 N 6 , Mr = 1176.07, orthorhombic, Cmca, Z = 4, a = 10.865(2) Å, b = 16.737(6) Å. c = 20.511(9) Å, V = 3730 Å 3 , d c  = 2.1 g·cm -3  measured at room temperature, R = 0.062 for 744 independent reflections and 100 L. S.-parameters. The solid contains bis[tris(dimethylamino)cyclohexadienylium]dications - obtained by dimerization of TDMAB +  radical cations - and triiodide counter anions. The solid is diamagnetic.

zeitschrift für naturforschung b

1,3,5-Tris(dimethylamino)benzol mit Iod und 1,3,5-Tricyanobenzol: Eine ungewöhnliche Dimerisierung und ein „normaler“ Donor/Akzeptor-Komplex / 1,3,5-Tris(dimethylamino)benzene with Iodine and 1,3,5-Tricyanobenzene: An Unusual Dimerization and a “Normal” Donor/Acceptor-Complex