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Discrete mononuclear TeCl -  5  anions were prepared for the first time in solid phase in association with bulky cations as tetrabutylammonium and tetraphenylphosphonium. The vibrational spectra imply tetragonal symmetry as for the isoelectronic TeF -  5  anion which is caused by a stereochemically active lone pair. A complete vibrational assignment is given and supported by a normal coordinate treatment for both ions. The significance of the resulting force constants is briefly discussed

Zur Existenz diskreter TeCl - 5 -Ionen / On the Existence of Discrete TeCl - 5 Ions