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[Ph 3 PN(H)Ph][AuI 2 ] (2) is formed by the reaction of AuI with N-Phenyl-iminotriphenylphosphorane, Ph 3 PNPh in a toluene suspension. 2,3-Bis(triphenylphosphinimino)maleic acid-N-methylimide (3) has been prepared by the Staudinger reaction of 2,3-bis(azido)maleic acid-N-methylimide with PPh 3  in THF solution in the form of red crystals. Crystal structure determinations of three iminophosphoranes were carried out by X-ray methods.

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Die Kristallstrukturen von Ph 3 PNPh, [Ph 3 PN(H)Ph][AuI 2 ] und von 2,3-Bis(triphenylphosphoranimino)maleinsäure-N-methylimid / The Crystal Structures of Ph 3 PNPh, [Ph 3 PN(H)Ph][AuI 2 ] and of 2,3-Bis(triphenylphosphoranimino)maleic Acid-N-methylimide