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Organodisulfide radical cations R2S2'® and R2C2S2'® can be generated from aliphatic as well as aromatic cyclic polysulfides in A1C13/H2CC12 solutions and characterized by their ESR spectra. Examples presented are the oxidations of 1,2,3-trithiolanes to 1,2-dithiolane radical cations, in which energetically favored planarized 3 electron/2 center bonds - S a r e formed.

Radical Ions, 78 [1, 2] The Oxidative Desulfuration of Organic Cyclic Polysulfides to Disulfide Radical Cations in AlCl 3 /H 2 CCl 2 Solution