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Mößbauer spectra of mono and dinuclear iron carbonyl complexes of three cyclic diazenes and the crystal structures of two products formed from (cis-diazene)Fe 2 (CO) 6  and alkynes are reported. The ring size of the diazene ligand influences the stereochemistry of the cycloadducts obtained in the latter reaction; the bicyclic diazaferracycloalkene skeleton of these compounds leads to an exo- and endo-arrangement of one iron carbonyl group relative to the five- and six- membered diazene, rcspectively.

zeitschrift für naturforschung b

Übergangsmetallkomplexe von Diazenen, XXIII [1]. Struktur und Mößbauer-Daten bi- und tricyclischer Ferracyclen / Transition Metal Complexes of Diazenes, XXIII [1] Structure and Mößbauer Data of Bi- and Tricyclic Ferracycles