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A transition metal induced C-C coupling by the reaction of W 2 (N(CH 3 ) 2 ) 6 , (4) and CS 2  yielded the zwitter ion S 2 C-C(N(CH 3 ) 2 ) 2  (1d) besides W 2 (N(CH 3 ) 2 ) 2 (CS 2 ) 2 S 4  (5). The com- plex chemistry of the zwitter ions 1d and S 2 CC(N(CH 2 ) 4 X) 2  (X = CH 2 , O) has been investigated by their reaction with (η 5 -C 5 H 5 ) 2 Mo 2 (CO) 4  (2) and (η 5 -C 5 H 5 )Mo(CO) 3 Cl (3). Reaction of the former led to complexes (η 5 -C 5 H 5 )Mo(CO) 2 (S 2 CR) (R = N(CH 3 ) 2 , N(CH 2 ) 4 X) and the new compounds [(η 5 -C 5 H 5 )Mo(CO) 2 (S 2 C-CR 2 )] + . X-ray structure analyses of 1d and ((η 5 -C 5 H 5 )Mo(CO) 2 (S 2 C-C(N(CH 2 ) 5 ) 2 )] ⊕ PF 6  ⊖  (10b) are described.

zeitschrift für naturforschung b

Darstellung und Charakterisierung des Zwitterions S 2 C—C(NMe 2 ) 2 ; eine übergangsmetallinduzierte C—C-Kopplung. Komplexchemie der Zwitterionen S 2 C—C(NR 2 ) 2  / Synthesis and Characterization of the Zwitter Ion S 2 C —C(NMe 2 ) 2 ; a Transition Metal Induced C —C Coupling. Complex Chemistry of the Zwitter Ions S 2 C —C(NR 2 ) 2