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The ionic conductivities (complex impedance measurements) of the olivine type Li 2 ZnCl 4 , Na 2 ZnCl 4  and Na 2 CoCl 4 , the Sr 2 PbO 4  type Na 2 MgCl 4 , Na 2 MnCl 4 , and Na 2 CdCl 4 , and the novel Na 2 CrCl 4  with monoclinically distorted Sr 2 PbO 4  structure (Na 2 CuF 4  type) are presented. The specific conductivities of Li2ZnCl4 and the Na2MCl4 are about three orders of magnitude lower than those of the fast ionic conducting lithium chloride spinels Li[LiM ]Cl 4  (M = Mg, Mn. Fe. Cd. etc.) indicating that in the latter compounds the tetrahedrally coordinated lithium ions exhibit higher mobility than those on octahedral sites. The X-ray data including those of Sr 2 PbO 4  type Na 2 TiCl 4  and both the IR and Raman spectra (together with a group theoretical treatment) are also given. The spectra obtained confirm the different structure types of the ternary chlorides.

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Ionic Conductivity, Structural, IR and Raman Spectroscopic Data of Olivine, Sr 2 PbO 4 , and Na 2 CuF 4  Type Lithium and Sodium Chlorides Li 2 ZnCl 4  and Na 2 MCl 4  (M = Mg, Ti, Cr, Mn, Co, Zn, Cd)