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(PhP) 5  and lithium dialkylamides in tetrahydrofuran form equilibrium mixtures of lithium aminophenylphosphides (PhP) n NR -  with n = 3 and (mainly) 2. The monophosphides (n = 1) are not formed; it is concluded that they are generally unstable, decomposing to aminodiphosphides and cyclophosphines. Alkylation of an equilibrium mixture gives 1-alkyl-2-dialkylamino-diphenyl- diphosphines which, however, are thermally unstable. (PhP) 5  degradation equilibria using differ­ent anionic nucleophiles are compared.

zeitschrift für naturforschung b

Dialkylamino-phenyldi- und -triphosphide aus dem (PhP) 5 -Abbau mit Alkaliamiden / Dialkylamino-phenyldi- and -triphosphides from the Degradation of (PhP) 5  by Alkali Amides