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Reaction of the tetrahydrofuran-stabilized 16-electron complex fragment [Cp*Re(CO) 2 ] with dimethyl disulfide, MeSSMe, leads to the diamagnetic title compound, Cp*Re(CO)(SMe) 2  , which was characterized by mass, IR and NMR spectra and by an X-ray crystal structure analysis**. The two methylsulfido ligands are bent (angles Re-S-CH 3  114.1(3)°) and turned away from the Cp* ring. The Re - S-bond distances are 227.0(2) pm.

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Darstellung, Charakterisierung und Röntgenstrukturanalyse von η 5  -Pentamethylcyclopentadienyl-bis(methylsulfido)carbonylrhenium, Cp*Re(CO)(SMe) 2  / Preparation, Characterization and X-Ray Structure Analysis of η 5 -Pentamethylcyclopentadienyl-bis(methylsulfido)carbonylrhenium, Cp*Re(CO)(SMe) 2