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The preparation of trithiadiazyl-hexafluoroarsenates by three different methods is reported: (a) reaction of S 3 N 2 Cl 2  (3) with AgAsF 6  (to give S 3 N 2 Cl +  ASF 6  - ), (b) halogen or radical addition to S 3 N 2  +  ASF 6  -  to give S 3 N 2 Br + AsF 6  -  (5) or S 3 N 2 ON(CF 3 ) 2  + ASF 6  -  (6), and (c) cycloaddition of NSF to the NS 2  +  -cation to give S 3 N 2 F + AsF 6  -  (9).

Trithiadiazyl-hexafluorarsenate S 3 N 2 X + AsF 6 - / Trithiadiazyl-hexafluoroarsenates S 3 N 2 X + AsF 6 -