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Trifluoromethyl azide decomposes in a low-pressure flow system at rather high temperatures by splitting off N 2 . The nature of the resulting products depends largely on the wall material of the pyrolysis tube: using molybdenum above 1120 K, FCN is observed exclusively. Neither F 2 C=NF nor F 3 C-N=N-CF 3  can be detected as intermediates by comparing their PE spectra with those continuously recorded while increasing the temperature. F 3 C-N = N - CF 3  fragments already at 870 K to give N 2  and F 3 C-CF 3 . The PE spectra of F 3 CN 3  and F 2 C=NF are assigned based on MNDO calculations

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Gasphasen-Reaktionen, 59 [1, 2] Die Pyrolysen von Trifluormethylazid und Hexafluorazomethan / Gas Phase Reactions, 59 [1, 2] The Pyrolyses of Trifluoromethylazide and Hexafluoroazomethane