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The crystal structures of LiGaCl 4  and LiGaI 4  have been determined by single crystal X-ray methods. Both compounds are isotypic with LiAlCl 4  and characterized by LiX 6  octahedra and GaX 4  tetrahedra. Mean bond lengths are: d̄(Ga-X) = 217.4 pm (Cl) and 255.9 pm (I); d̄(Li-X) = 263.9 pm (Cl) and 305.3 pm (I), respectively. Common features of the isotypic compounds LiGaX 4  (X = Cl, Br. I) are discussed.

Darstellung und Kristallstrukturen von LiGaCl4 und LiGaI4/ Preparation and Crystal Structure of LiGaCL 4 and LiGaI 4