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The following mixed ligand complexes were synthesized and characterized: Co(Phdtcz) 2 (Phtu) 2 , Co(Phdtcz) 2 (Clphtu) 2  , Co(Phdtcz) 2 (dtm), Ni(Et 2 dtc) 2 (dtm), Ni(Phdtc) 2 (dtm), Ni(p-Toluiddtc) 2 (dtm), Ni(α-naphdtc) 2 (dtm), and Ni(Phdtcz)(Et 2 dtc); where Phdtcz = phenyldithiocarbazate, Et 2 dtc = diethyldithiocarbamate, Phdtc = phenyldithiocarbamate, p-Toluiddtc = p-toluidinedithiocarbamate, α-naphdtc = α-naphthyldithiocarbamate, Phtu = phenylthiourea, Clphtu - chlorophenylthiourea, and dtm - bis(diphenylphosphinothioyl)-methane. Electronic and IR spectra, magnetic, conductivity and X-ray powder diffraction measurements were carried out. The Ni(II) and Co(II) complexes are suggested to be square planar and octahedral, respectively. The biological activity of the complexes was also tested.

Reactivity of 1,1-DithioIato Ni(II) and Co(II) with Phenylthiourea, Chlorophenylthiourea and Bis(diphenylphosphinothioyl)methane