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The σ-ferrocenyl complex CpW (NO) 2 Fc (1) was prepared from CpW (NO) 2 Cl and ferrocenyl lithium, and oxidized by air in CH 2 Cl 2  solution to give CpWO 2 Fc (2). An X-ray crystal structure analysis of 1 indicated the presence of two almost linear nitrosyl groups (with W -N -O angles of 173.0(9) and 175.4(7)°). The W -C (ferrocenyl) bond length is 2.164(10) Å.

zeitschrift für naturforschung b

Darstellung und Molekülstruktur des Ferrocenylkomplexes CpW(NO) 2 Fc und seine Oxidation zu CpWO 2 Fc/Synthesis and Molecular Structure of the Ferrocenyl Complex CpW(NO) 2 Fc and its Oxidation to CpWO 2 Fc