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Spectra and Crystal Structures of the Adducts C l5Sb • [N(/-C3H 7)C N (i-C3H 7)] and C l4Sn • 2 [N(/-C3H 7)CN(/-C3H 7)j X-Ray, Vibrational Data, Diisopropylcarbodiimide Adducts of SbCl5, SnCl4 Thecarbodiimide adducts Cl5Sb &lt;-(—N (R) = C = N R)(1) and Cl4S n ^ (-N (R) = C = N R) 2(2)(R = /-C3H 7) have been prepared by the reaction o f R —N = C —N — R with SbCl5 in a 1:1 and with SnCl4 in a 2:1 molar ratio, respectively. The vibrational spectra (IR and Raman) of both compounds have been regarded and assigned to the skeleton modes. The X-ray structure determination shows the orthorhombic space group Pna2, with 4 formula units per unit cell for 1. Adduct 2 has a trans-configuration and crystallizes in the triclinic space group P 1 with only one molecule per unit cell.

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Die Spektren und Kristallstrukturen der Addukte CI 5 Sb · [N(i-C 3 H 7 )CN(i-C 3 H 7 )] und Cl 4 Sn · 2 [N(i-C 3 H 7 )CN(i-C 3 H 7 )] / Spectra and Crystal Structures of the Adducts Cl 5 Sb · [N(i-C 3 H 7 )CN(i-C 3 H 7 )] and Cl 4 Sn · 2 [N(i-C 3 H 7 )CN(i-C 3 H 7 )]