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S 5 N 5 [SnCl 5 (CH 3 CN)] is prepared by the reaction of SnCl 2  with trithiazyl chloride in acetonitrile suspension. The compound is characterized by its IR spectrum, the  119 Sn Mössbauer spectrum and by an X-ray crystal structure determination (1851 observed, independent reflexions, R = 0.024). S 5 N 5 [SnCl 5 (CH 3 CN)] crystallizes in the monoclinic space group P2 1 /n with Z = 4 and the lattice dimensions a = 758.8; b = 1574.6; c = 1429.1 pm; β = 97.65°. The compound consists of planar S 5 N 5  ®  cations with the azulene-like structure, and anions [SnCl 5 (CH 3 CN)]e in which the tin atom has a distorted octahedral coordination. The bond angle Sn-N ≡ C (168°) is surprisingly small.

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S 5 N 5 [SnCl 5 (CH 3 CN)]; Synthese, IR-Spektrum,  119 Sn-Mößbauer-Spektrum und Kristallstruktur / S 5 N 5 [SnCl 5 (CH 3 CN)]; Synthesis, IR Spectrum , Mössbauer Spectrum and Crystal Structure