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[WCl 3 (N 3 S 2 )(pyridine)] was obtained by the reaction of a mixture of S 5 N 5 [WCl 4 (N 3 S 2 )] and S 4 N 3 [WCl 4 (N 3 S 2 )] with pyridine in dichloromethane. It forms brown, moisture-sensitive crystal plates and was characterized by its IR spectrum and an X-ray crystal structure determination (1404 ob­served reflexions. R = 0.052). Crystal data: ortho­rhombic, space group Pbca. Z = 8, a = 708.3, b = 1275.4, c = 2628.6 pm. The tungsten atom has a distorted octahedral coordination and is part of a planar WN 3 S 2  ring with WN bond lengths of 176 and 186 pm. The pyridine ligand (W−N 232 pm) is in trans position to the shorter WN bond.

Synthese und Kristallstruktur von [WCl 3 (N 3 S 2 )(Pyridin)] / Synthesis and Crystal Structure of [WCl 3 (N 3 S 2 )(Pyridine)]