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The title compound was prepared by reaction of aqueous solutions of Ba(SCN) 2  • 3 H 2 O and CdSO 4  • 8/3 H 2 O in the molar ratio of 3:1. The crystal structure was solved by X-ray methods (M r  = 861.61, space group P 2 1 /c, Z = 4, a = 943.6(3) pm, b = 1469.7(6) pm, c = 1827.1(6) pm, β = 109.02(7), V = 2395.4 10 6  pm 3 , λ (AgKa) = 55.83 pm, d c  = 2.38 gcm -3 , μ(AgKa) = 22.4 cm -1 , F(000) = 1591.9, T = 298 K, final R = 0.035 for 1350 independent reflexions). The structure consists of two crystallographically independent, distorted Cd(SCN) 6  octahedra. Both crystallographically different Ba 2+  cations are surrounded by 4 oxygen atoms of water and 5 nitrogen atoms of SCN, forming chains in the direction o f the b-axis

zeitschrift für naturforschung b

Zur Koordination von Thiocyanat in ternären Metallkomplexen Die Kristallstruktur von Ba 2 Cd(SCN) 6  • 7 H 2 O / On the Coordination of Thiocyanate in Ternary Metal Complexes The Crystal Structure of Ba 2 Cd(SCN) 6  • 7 H 2 O