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The complex salt [Ni(C 2 H 6 N 4 O 2 ) 2 ][Pt(C 2 O 4 ) 2 ] × [Νi(C 2 Η 5 Ν 4 O 2 ) 2 ] × 2 H 2 O has been crystal­lized by interdiffusion of [Ni(C 2 H 6 N 4 O 2 ) 3 ]Cl 2  and K 2 [Pt(C 2 O 4 ) 2 ]. It is triclinic. Ρ1̄. a = 3.673(1), b = 13.622(4), c = 14.371(4) Å, α = 94.01(2), β = 95.11(2), γ = 92.14(2)°. V = 713.7(4) Å 3 , Z = 1, M r  = 994.96, D x  = 2.31 g cm -3 , MoK α , γ = 0.710 Å. μ = 61.3 cm -1 , F(000) = 488, room temperature, wR = 0.034 for 3109 observed independent reflections. Segregated parallel stacksof [Pt(C 2 O 4 ) 2 ] 2 - anions, [Ni(C 2 H 6 N 4 O 2 ) 2 ] 2+  cations, and neutral [Ni(C 2 H s N 4 O 2 ) 2 ] complex molecules run along a, and there is a 2:1 ratio of Ni and Pt complex stacks, interlinked by a network of strong intermolecular H bridges. The difference between the double positive and the neutral Ni complexes is marginal, as the assignment of the charges is based upon a slightly asymmetric intermolecular Ο-H--O bridge. 1.06(7) and 1.44(8) Å.

zeitschrift für naturforschung b

[Bis(oxamidoxim)nickeI(II)]-[Bis(oxalato)platinat(II)]-Dihydrat x [Bis(oxamidoximato)nickel(II)]: Getrennte parallele Stapel im Verhältnis 2:1 / [Bis(oxamide oxime)nickel(II)] [Bis(oxalato)platinate(II)] Dihydrate x [Bis(oxamide oximato)nickel(II)]: Segregated Parallel Stacks in the Ratio 2:1