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The compounds  t C 4 H 9 N=VR(O t C 4 H 9 ) 2  (R = CH 3 ,  n C 4 H 9 , CH 2 SiMe 3 , Mes) and  t C 4 H 9 N = VMes 2 (O t C 4 H 9 ) have been prepared by reaction of tert-butyliminovanadium (V) chlorides with LiR;  t C 4 H 9 N=V(CH 2 SiMe 3 ) 2 (O t C 4 H 9 ) and  t C 4 H 9 N=VR 3  (R = CH 2 SiMe 3 , Mes) could only be characterized by NMR spectroscopy. The  1 H,  13 C and  51 V NMR spectra are discussed; the constants of  51 V ,  14 N coupling have been determined.

zeitschrift für naturforschung b

tert-Butylimino-δ-Organovanadium(V)-Verbindungen Darstellung und NMR-spektroskopische Untersuchungen/tert-Butylimino-δ-Organovanadium (V) Compounds Synthesis and NMR Spectroscopic Studies