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The reaction of MoCl 3 (THF) 3  with PhP(CH 2 CH 2 CH 2 PPh 2 ) 2  in THF/CH 2 Cl 2  gave MoCl 3 (PhP(CH 2 CH 2 CH 2 PPh 2 ) 2 ) ·CH 2 CI 2  (1). Sodium amalgam reduction of I in the presence of the monotertiary phosphines PMe 3-n Ph n  (n = 0, 1, 2), in THF under nitrogen atmosphere, yielded the bis(dinitrogen) complexes

zeitschrift für naturforschung b

Oligophosphan-Liganden, XIV [1] Bis(distickstoff)molybdän-KomplexeMo(N 2 ) 2 [PhP(CH 2 CH 2 CH 2 PPh 2 ) 2 ](PR 3 ) / Oligophosphine Ligands, XIV [1] Bis(dinitrogen)molybdenum Complexes Mo(N 2 ) 2 [PhP(CH 2 CH 2 CH 2 PPh 2 ) 2 ](PR 3 )