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Chlorodiphenylphosphane and triethylammonium perfluoropinacolate yield the monocyclic hydrophosphorane 3. The X-ray structure analysis reveals that hydrogen is bonded in the axial position of a trigonal bipyramide. With dimethyl sulfoxide 3 undergoes a ring opening reaction to give phosphinate 5.

zeitschrift für naturforschung b

Ein monocyclisches Phosphoran mit axial gebundenem Wasserstoff: Darstellung und Molekülstruktur / A Monocyclic Phosphorane with Hydrogen in Axial Position: Preparation and Molecular Structure