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The iminovanadium (V) com pounds  t C 4 H 9 N = V(N t C 4 H 9 -SiMe 2 -NH t C 4 H 9 )Cl 2  (3) and [VCl(μ-Cl)(N t C 4 H 9 )(NH t C 4 H 9 )(NH 2  t C 4 H 9 )] 2  have been prepared by reaction of Me 2 Si(NH t C 4 H 9 ) 2  with VO(OC 2 H 5 )Cl 2  and VO(O  t C 3 H 7 )Cl 2 , respectively. 3 was investigated by  1 H ,  51 V NMR spectroscopy and X-ray diffraction analysis; the structure has been found to be a mononuclear vanadium complex with a distorted trigonal bipyramidal arrangement of the ligands.

zeitschrift für naturforschung b

Reaktion der Alkoxo-oxovanadium(V)-dichloride mit Bis(tert-butylamino)-dimethylsilan/ Reaction of Alkoxo Oxovanadium(V) Dichlorides with Bis(tert-butylamino) Dimethylsilane