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Cyanides such as P(CN) 3  , As(CN) 3  , PhP(CN) 2  , Bu t As(CN) 2  and Ge(CN) 4  react with [(CF 3 ) 2 CS] 2  (1) by insertion of the carbon atom of the iso-nitrile isomer into the four-membered [CS] 2  ring to give compounds PR′ 3  (2), AsR′ 3  (3), FP(S)R′ 2  (4), PhP(S)R′2 (5), Bu t AsR′ 2  (6) and GeR′ 4  (7) respectively, where R′ is the novel heterocyclic ligand[xxx]. The crystal structures of 3 and 7 are reported.

Reactions of the Hexafluorothioacetone Dimer with Cyanides of Phosphorus, Arsenic and Germanium