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Diastereomeric mixtures for members of series CH 3  (t-C 4 H 9 )P(X ) -Y -(Z)P(t-C 4  H 9 )CH 3  were prepared. Pure meso- and rac-[CH 3  (t-C 4 H 9 )P (S)] 2  (8a/8b) and rac-[CH 3  (t-C 4 H 9 )P(S)] 2 S (13) were isolated. Exchange reactions leading to redistribution of sulfur between tri- and pentavalent phosphorus sites are discussed. A novel one-batch method is used for the synthesis of diphosphine disulfides.

Diastereomere Organophosphorverbindungen, I Darstellung und Eigenschaften von CH 3 (t-C 4 H 9 )P(X)—Y —(Z)P(t-C 4 H 9 )CH 3