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[Fe(2,2'-bpy) 3 ][Fe 2 OCl 6 ] is obtained in form of red, air stable crystals by oxidation of Fe(bpy)Cl 2  with O 2  in acetonitrile. It crystallizes in the monoclinic space group P2 1 /c with Z = 4. The crystal structure contains Fe(bpy) 3  2+  and Fe 2 OCl 6  2-  ions. The anion exhibits a bent oxobridge with Fe-O-Fe = 148,1° and Fe-O distances of equal length (176,5 pm). In the IR spectrum ν as  Fe-O-Fe is observed at 850 cm -1 , the Fe-Cl valence vibrations at 362 and 317 cm  -1 .

Synthese und Kristallstruktur von Tris(2,2'-bipyridin)eisen(II) μOxo-bis(trichloroeisen(III)), ein Salz mit dem Anion Fe 2 OCl 6 2-