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Polymeric phosphono-vanadates M I[ CH 3 PVO 5 ]·H 2 O (M=K, NH 4 ) and the acid H[CH 3 PVO 5 ]·H 2 O have been prepared. K[CH 3 PVO 5 ]·H 2 O crystallizes in the trigonal space group P3 1 21 with a = 1111.2(2) and c = 1004.0(3) pm, and consists of an open structure of corner sharing V-O- and CH 3 -P-O-polyhedra. Polyhedral chains form helices along the screw axis of the space group. The vanadium polyhedron can be described as highly distorted trigonal bipyramid with two terminal oxygen atoms.

Polymere Methylphosphono-vanadate: Struktur von K[CH 3 PVO 5 ]·H 2 O / Polymeric M ethylphosphono Vanadates: Structure of K[CH 3 PVO 5 ]·H 2 O