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ReNF 4  · ReF 5 (NCl) is prepared by direct fluorination of ReNCl 4  with fluorine between 80 °C and 130 °C. The red crystals are extremely sensitive to moisture. The complex is characterized by the IR spectrum and by an X-ray structural investigation. ReNF 4  · ReF 5 (NCl) crystallizes orthorhombically in the space group Pnma with 4 formula units per unit cell and with the cell dimensions  a =  1440,  b =  848,  c =  776 pm (419 observed, independent reflexions,  R =  13.9%). The complex consists of the molecules ReNF 4  and ReF 5 (NCl), which are linked by a linear asymmetric fluorine bridge. The bridging fluorine atom is in trans-position to the nitrido ligand Re -F - 228 pm) and to the nitreno ligand (Re -F = 159 pm and Re= N - Cl 164 pm) correspond to triple 188 pm). The Re ≡ N bond lengths Re= N bonds.

ReNF 4 · ReF 5 (NCl), ein Nitrido-Nitrenokomplex von Rhenium(VII)/ ReNF 4 · ReF 5 (NCl), a Nitrido Nitrene Complex of Rhenium (VII)