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Mo 2 O 4 Cl 2 (bipy) 2  has been obtained by oxidation of MoCl 4 (bipy) with O 2  in ethanol/H 2 O . The complex crystallizes from CH 3 NO 2  with one solvent molecule per formula unit in the monoclinic space group P 2 1 /n: a = 954.1(2), b = 1925.3(2), c = 1423.2(2) pm, β = 102.48(2)°, Z = 4. The characteristic unit Mo 2 O 4  2+  of the dinuclear complex consists of two terminal oxo ligands in a cisarrangem ent and two bridging oxygen atoms forming a non-planar Mo 2 O 2  ring. A strong Mo -Mo single bond is indicated by a short distance of 256.5 pm. The coordination of both Mo atoms is completed by a Cl atom and a chelating bipyridyl ligand.

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Die Kristallstruktur von Di-μ-oxo-cis-dioxo-dichloro-bis(2,2′ -bipyridyl)- molybdän(V) (Mo–Mo)-Nitromethansolvat, Mo 2 O 4 Cl 2 (bipy) 2  · CH 3 NO 2 / Crystal Structure of Di-μ-oxo-cis-dioxo-dichloro-bis(2,2′-bipyridyl)- molybdenum(V) (Mo–Mo) Nitromethane Solvate, Mo 2 O 4 Cl 2 (bipy) 2  ´ CH 3 NO 2