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Synthesis and properties of tris(phosphane)(ethene)nickel(0) complexes (dmpe)(PR 3 )Ni(C 2 H 4 ) (R = CH 3 (4), c-C 6 H 11 (5), and C 6 H 5  (6)) are reported. In solution. 4-6 are thermolabile and undergo ligand exchange reactions affording tetrakis(phosphane)nickel(0 ) and bis(phosphane)- (ethene)nickel(0) complexes.  1 H,  13 C, and  31 P NMR data of 4-6 confirm the tetrahedral geometry around nickel. For 6 , the crystal and molecular structure has been determined by X-ray crystallography.

zeitschrift für naturforschung b

Tris(phosphan)-Nickel(0)-Ethen-Komplexe (dmpe)(PR 3 )Ni(C 2 H 4 ). Molekülstruktur des (dmpe)(PØ 3  )Ni(C 2 H 4 )/ Tris(phosphane)-nickel(0)-ethene Complexes (dmpe)(PR 3 )Ni(C 2 H 4 ). Molecular Structure of (dmpe)(PO 3 )Ni(C 2 H 4 )