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A series of dithiocarbimato complexes (R 3 P) 2 M(S 2 CNR′) (1, 2) has been obtained by reaction of (R 3 P) 2 MCl 2  (M = Pd, Pt) with primary amines and carbon disulfide. The dithiocarbimato complexes 1 and 2 can be reversibly protonated to give the dithiocarbamato compounds (R 3 P) 2 M[S 2 CN(H)R′] + Cl - .

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Reaktionen von Übergangsmetall-Verbindungen mit primären Aminen und Schwefelkohlenstoff: Dithiocarbimato- und Dithiocarbamato-Komplexe von Palladium, Platin, Nickel, Cobalt und Gold. Röntgenstruktur von (Et 3 P) 2 MS 2 CNCH 2 Ph (M = Pd, Pt) / Reactions of Transition Metal Compounds with Primary Amines and Carbon Disulfide: Dithiocarbimato and Dithiocarbamato Complexes of Palladium, Platinum, Nickel, Cobalt and Gold. X-Ray Structure of (Et 3 P) 2 MS 2 CNCH 2 Ph (M = Pd, Pt)