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The anodic deposition of Pb 8 Tl 5 O 24  is compared with that one of Tl 2 O 3  and α-PbO 2 . Scanning electron microscopic pictures of the oxide surfaces show obvious differences. This should be the reason for different oxygen overpotentials measured at these anodes. Comparative cyclic voltammograms show, that the redox behaviour of Pb 8 Tl 5 O 24  in sulfuric acid is essentially determined by the lead ions. Because of the high corrosion rate Pb 8 Tl 5 O 24  is not suitable as anode material for electrolysis in sulfuric acid

zeitschrift für naturforschung b

Vergleichende Untersuchungen an Pb 8 Tl 5 O 24 -, α-PbO 2 - und Tl 2 O 3 -Elektroden / Comparative Investigations of Pb 8 Tl 5 O 24 , α-PbO 2  and Tl 2 O 3  Electrodes